Structures by: Batke S.

Total: 67

C28H33F3N3O3PSZr

C28H33F3N3O3PSZr

Sietzen, MalteBatke, SonjaMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2015) 34, 6 1118

a=17.62850(16)Å   b=10.81736(10)Å   c=30.9896(3)Å

α=90°   β=90°   γ=90°

C45H38ClNP2Zr,C4H10O

C45H38ClNP2Zr,C4H10O

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=12.1149(2)Å   b=12.1996(2)Å   c=28.4817(4)Å

α=90°   β=91.1112(15)°   γ=90°

C38H32I3NP2Zr,1.5(CH2Cl2)

C38H32I3NP2Zr,1.5(CH2Cl2)

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=12.32855(16)Å   b=12.57691(19)Å   c=15.78601(14)Å

α=104.1686(10)°   β=96.0145(9)°   γ=116.0700(14)°

C38H32HfI3NP2,C7H8

C38H32HfI3NP2,C7H8

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=12.3761(2)Å   b=17.07238(16)Å   c=20.1630(3)Å

α=90°   β=101.9429(13)°   γ=90°

C41.75H41Cl3NP2Zr

C41.75H41Cl3NP2Zr

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=11.44486(13)Å   b=17.6843(2)Å   c=19.9828(3)Å

α=80.0131(11)°   β=88.4840(10)°   γ=72.8933(10)°

C62H69BNP2Zr

C62H69BNP2Zr

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=17.3823(5)Å   b=17.7265(5)Å   c=21.7567(5)Å

α=67.552(2)°   β=66.932(2)°   γ=66.047(3)°

C38H32I3NP2Zr,CH2Cl2

C38H32I3NP2Zr,CH2Cl2

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=12.220(5)Å   b=16.920(7)Å   c=19.864(9)Å

α=90°   β=106.052(10)°   γ=90°

C44H50HfN4P2

C44H50HfN4P2

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=12.47419(13)Å   b=12.67913(18)Å   c=14.64329(19)Å

α=81.2172(11)°   β=85.5974(9)°   γ=61.4891(12)°

C47H45ClNO0.5P2Zr

C47H45ClNO0.5P2Zr

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=18.9791(3)Å   b=11.12020(16)Å   c=38.2266(5)Å

α=90°   β=101.1276(14)°   γ=90°

C38H33NP2

C38H33NP2

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=10.66534(12)Å   b=12.26799(17)Å   c=13.52930(18)Å

α=111.4620(12)°   β=107.2399(11)°   γ=96.1928(10)°

C45H38ClHfNP2,C4H10O

C45H38ClHfNP2,C4H10O

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=12.05585(7)Å   b=12.17458(6)Å   c=28.6103(2)Å

α=90°   β=91.9077(6)°   γ=90°

C52H45NP2Zr

C52H45NP2Zr

Sietzen, MalteBatke, SonjaAntoni, Patrick W.Wadepohl, HubertBallmann, Joachim

Dalton Trans. (2017)

a=14.04739(15)Å   b=12.35375(14)Å   c=28.0234(3)Å

α=90°   β=98.1365(10)°   γ=90°

C24H27Cl2N2PTi

C24H27Cl2N2PTi

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=8.314(3)Å   b=19.255(8)Å   c=15.270(7)Å

α=90°   β=104.617(8)°   γ=90°

C24H27Cl2HfN2P,CH2Cl2

C24H27Cl2HfN2P,CH2Cl2

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=8.58828(12)Å   b=11.7688(2)Å   c=14.5396(3)Å

α=66.6471(16)°   β=84.8482(13)°   γ=75.6062(13)°

C30H47N4PSi2Zr

C30H47N4PSi2Zr

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=10.232(4)Å   b=11.587(5)Å   c=15.894(7)Å

α=87.520(8)°   β=74.549(10)°   γ=66.993(11)°

C30H47HfN4PSi2

C30H47HfN4PSi2

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=10.220(5)Å   b=11.565(7)Å   c=15.890(9)Å

α=87.543(9)°   β=74.477(8)°   γ=67.140(11)°

C24H35Cl2N2PTi

C24H35Cl2N2PTi

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=13.8960(3)Å   b=20.0990(4)Å   c=9.01231(14)Å

α=90°   β=90°   γ=90°

C24H35Cl2HfN2P

C24H35Cl2HfN2P

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=10.516(4)Å   b=29.311(11)Å   c=9.277(4)Å

α=90°   β=114.210(9)°   γ=90°

C38H49N2PZr

C38H49N2PZr

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=16.53716(5)Å   b=19.78721(7)Å   c=20.54069(9)Å

α=90°   β=90°   γ=90°

C29H39N4PTi

C29H39N4PTi

Sietzen, MalteBatke, SonjaMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2015) 34, 6 1118

a=8.48075(19)Å   b=12.3163(2)Å   c=13.7435(3)Å

α=81.9190(17)°   β=81.3926(18)°   γ=70.9432(19)°

C30H48N3PSi3

C30H48N3PSi3

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=10.1543(3)Å   b=33.3760(7)Å   c=10.6730(3)Å

α=90°   β=104.838(3)°   γ=90°

C34H53Li2N3OPSi3,C16H36LiO4

C34H53Li2N3OPSi3,C16H36LiO4

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=9.609(8)Å   b=16.534(12)Å   c=18.232(15)Å

α=103.949(9)°   β=92.390(17)°   γ=95.127(8)°

C32H51N4PSi3Zr

C32H51N4PSi3Zr

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=11.604(6)Å   b=11.970(6)Å   c=15.902(7)Å

α=92.052(11)°   β=109.865(9)°   γ=118.711(11)°

C32H51HfN4PSi3

C32H51HfN4PSi3

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=11.58910(9)Å   b=11.99210(11)Å   c=15.93941(10)Å

α=92.1162(6)°   β=109.7773(6)°   γ=118.7552(9)°

C31H45F3HfN3O3PSSi3

C31H45F3HfN3O3PSSi3

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=18.1196(8)Å   b=21.4503(11)Å   c=19.9812(11)Å

α=90°   β=105.836(5)°   γ=90°

C30H45ClN3PSi3Ti

C30H45ClN3PSi3Ti

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=11.273(5)Å   b=16.455(7)Å   c=19.074(9)Å

α=90°   β=106.134(6)°   γ=90°

C30H45ClN3PSi3Zr

C30H45ClN3PSi3Zr

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=11.408(5)Å   b=16.448(7)Å   c=19.168(10)Å

α=90°   β=105.986(17)°   γ=90°

C30H45ClHfN3PSi3

C30H45ClHfN3PSi3

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=11.40019(6)Å   b=16.50065(7)Å   c=19.14401(10)Å

α=90°   β=105.9686(5)°   γ=90°

C30H46Cl2N3PSi3Ti

C30H46Cl2N3PSi3Ti

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=9.7694(5)Å   b=11.3071(4)Å   c=18.5921(7)Å

α=107.384(3)°   β=101.288(4)°   γ=92.178(3)°

C37H53ClN3PSi3Ti

C37H53ClN3PSi3Ti

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=20.2970(4)Å   b=9.31074(14)Å   c=22.7693(5)Å

α=90°   β=112.201(3)°   γ=90°

C48H54Cl2N6P2Si2Ti3,3(C6D6)

C48H54Cl2N6P2Si2Ti3,3(C6D6)

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic chemistry (2014) 53, 8 4144-4153

a=15.4536(4)Å   b=15.5687(4)Å   c=15.9472(4)Å

α=74.457(2)°   β=66.589(3)°   γ=68.283(2)°

C24H27Cl2N2PZr,CH2Cl2

C24H27Cl2N2PZr,CH2Cl2

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=8.582(3)Å   b=11.757(5)Å   c=14.513(5)Å

α=66.612(7)°   β=84.723(8)°   γ=75.566(12)°

C26H35HfI2N2PSi2

C26H35HfI2N2PSi2

Batke, S.Kothe, T.Haas, M.Wadepohl, H.Ballmann, J.

Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3528-3540

a=11.107(4)Å   b=19.914(8)Å   c=14.621(6)Å

α=90°   β=102.102(10)°   γ=90°

C36H37N2P

C36H37N2P

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=17.735(11)Å   b=12.421(7)Å   c=27.719(17)Å

α=90°   β=106.880(16)°   γ=90°

C40H47N4PZr,C2.5H6

C40H47N4PZr,C2.5H6

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=18.9485(3)Å   b=13.7692(2)Å   c=30.4136(5)Å

α=90°   β=105.8995(17)°   γ=90°

C40H47HfN4P

C40H47HfN4P

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=11.336(5)Å   b=13.390(5)Å   c=14.599(5)Å

α=102.302(13)°   β=102.584(12)°   γ=110.230(10)°

C36H39N4PTi

C36H39N4PTi

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=9.060(5)Å   b=11.614(5)Å   c=15.921(7)Å

α=81.263(16)°   β=89.363(8)°   γ=70.231(9)°

C40H47N4PTi

C40H47N4PTi

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=11.32651(18)Å   b=13.3144(2)Å   c=14.6393(3)Å

α=102.6184(16)°   β=102.3519(15)°   γ=110.2763(15)°

C32H27I2N2PTi

C32H27I2N2PTi

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=11.75732(8)Å   b=14.56140(10)Å   c=17.37463(12)Å

α=90°   β=102.2165(7)°   γ=90°

C36H35I2N2PTi,C7H8

C36H35I2N2PTi,C7H8

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=12.83406(11)Å   b=13.50260(12)Å   c=22.40089(18)Å

α=90°   β=96.3526(8)°   γ=90°

C32H27I2N2PZr,C6D6

C32H27I2N2PZr,C6D6

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=16.0851(2)Å   b=10.29017(12)Å   c=21.1915(2)Å

α=90°   β=96.7080(12)°   γ=90°

C32H27I2N2PZr,C7H8

C32H27I2N2PZr,C7H8

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=16.0977(3)Å   b=10.43778(18)Å   c=21.0529(3)Å

α=90°   β=92.9851(13)°   γ=90°

C26H35I2N2PSi2Zr

C26H35I2N2PSi2Zr

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=11.15467(11)Å   b=19.96395(19)Å   c=14.66400(15)Å

α=90°   β=102.0437(10)°   γ=90°

C36H35I2N2PZr

C36H35I2N2PZr

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=21.784(11)Å   b=11.603(5)Å   c=27.779(13)Å

α=90°   β=90.962(7)°   γ=90°

C36H35HfI2N2P

C36H35HfI2N2P

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=22.0703(2)Å   b=11.52011(9)Å   c=29.7547(2)Å

α=90°   β=99.6396(9)°   γ=90°

C40H49N2PSi2Zr

C40H49N2PSi2Zr

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=10.3850(2)Å   b=10.8151(3)Å   c=18.4097(5)Å

α=73.997(2)°   β=89.0580(18)°   γ=74.023(2)°

C40H49HfN2PSi2

C40H49HfN2PSi2

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=10.4057(3)Å   b=10.8811(4)Å   c=18.4072(5)Å

α=74.352(3)°   β=89.204(3)°   γ=73.940(3)°

C40H49HfN2PSi2

C40H49HfN2PSi2

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=10.25124(15)Å   b=39.7877(5)Å   c=10.27791(15)Å

α=90°   β=117.9006(19)°   γ=90°

C40H49HfN2PSi2,C4H10O

C40H49HfN2PSi2,C4H10O

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=14.1757(2)Å   b=16.0067(3)Å   c=20.6655(5)Å

α=69.808(2)°   β=84.7664(16)°   γ=85.5702(15)°

C46H41N2PZr

C46H41N2PZr

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=10.2300(3)Å   b=13.3848(3)Å   c=16.6135(3)Å

α=67.695(2)°   β=86.916(2)°   γ=86.495(2)°

C46H41HfN2P

C46H41HfN2P

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=9.69030(19)Å   b=13.2661(3)Å   c=15.1478(4)Å

α=100.832(2)°   β=92.9449(19)°   γ=101.4852(17)°

C50H49HfN2P

C50H49HfN2P

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=24.105(13)Å   b=17.206(9)Å   c=22.372(11)Å

α=90°   β=99.948(8)°   γ=90°

C72H70N4P2Zr,C5H12

C72H70N4P2Zr,C5H12

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=20.2073(7)Å   b=14.3395(4)Å   c=23.1834(7)Å

α=90°   β=107.080(4)°   γ=90°

C64H59N4PZr

C64H59N4PZr

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=15.3382(3)Å   b=13.3600(3)Å   c=25.6716(5)Å

α=90°   β=104.950(2)°   γ=90°

C49H58HfN3PSi2

C49H58HfN3PSi2

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=11.21305(9)Å   b=17.74642(13)Å   c=22.97468(19)Å

α=98.1474(6)°   β=91.2024(7)°   γ=98.6327(6)°

C68H67HfN4P,C2H5O0.5

C68H67HfN4P,C2H5O0.5

Batke, SonjaSietzen, MalteMerz, LukasWadepohl, HubertBallmann, Joachim

Organometallics (2016) 35, 13 2294

a=11.84756(13)Å   b=12.4209(2)Å   c=20.4206(3)Å

α=107.3504(15)°   β=93.0867(11)°   γ=95.0282(11)°

0.5(C44H53Li2N2O2P),0.5(C44H52Li2N2O2P),0.5(C4H9O)

0.5(C44H53Li2N2O2P),0.5(C44H52Li2N2O2P),0.5(C4H9O)

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=12.0189(2)Å   b=23.7073(4)Å   c=15.0077(3)Å

α=90°   β=97.4873(16)°   γ=90°

C39H37F3N2O3PSTa

C39H37F3N2O3PSTa

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=10.24496(17)Å   b=18.6808(4)Å   c=19.1934(4)Å

α=82.1604(16)°   β=82.5253(15)°   γ=89.5979(15)°

C36H38N4PTa

C36H38N4PTa

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=10.75983(15)Å   b=18.5817(2)Å   c=15.9528(2)Å

α=90°   β=97.7237(13)°   γ=90°

C37H40N2PTa

C37H40N2PTa

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=8.697(4)Å   b=9.920(4)Å   c=22.130(11)Å

α=101.690(8)°   β=95.415(13)°   γ=99.097(9)°

C42H48N2PSiTa

C42H48N2PSiTa

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=11.57180(14)Å   b=12.44923(14)Å   c=14.67713(17)Å

α=90.3798(9)°   β=101.0855(10)°   γ=104.7680(10)°

C44H56N2PSi2Ta,C7H8

C44H56N2PSi2Ta,C7H8

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=13.0048(3)Å   b=14.5179(3)Å   c=14.9384(3)Å

α=94.6661(18)°   β=115.584(2)°   γ=108.750(2)°

C43H53N2P2SiTa,C4H10O

C43H53N2P2SiTa,C4H10O

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=9.39598(8)Å   b=21.86855(18)Å   c=22.49629(19)Å

α=87.6364(7)°   β=82.5388(7)°   γ=84.0719(7)°

C46H60N2P3SiTa,C6D6

C46H60N2P3SiTa,C6D6

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=11.08257(12)Å   b=11.90731(11)Å   c=20.8619(2)Å

α=96.7192(8)°   β=103.3852(9)°   γ=110.8123(9)°

C42H50N2P3Ta

C42H50N2P3Ta

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=10.20187(4)Å   b=22.75735(6)Å   c=17.01422(5)Å

α=90°   β=102.6140(3)°   γ=90°

C36H34I2N2PTa,0.33(C4H10O),0.17(C7H7)

C36H34I2N2PTa,0.33(C4H10O),0.17(C7H7)

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=12.964(7)Å   b=16.745(9)Å   c=29.705(15)Å

α=76.866(11)°   β=86.362(18)°   γ=71.547(12)°

C76H68F12N4O12P2S4Ta2,3(C7H8)

C76H68F12N4O12P2S4Ta2,3(C7H8)

Batke, SonjaSietzen, MalteWadepohl, HubertBallmann, Joachim

Inorganic Chemistry (2017)

a=13.8800(2)Å   b=19.0045(4)Å   c=20.1978(3)Å

α=74.5788(15)°   β=89.5752(13)°   γ=72.9103(16)°